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How to calculate benzimidazole yield from o-phenylenediamine?
Cool the filtrate to about 10 °C, filter off the benzimidazole, wash with 25 ml of cold water and dry at 100 °C. The yield of pure benzimidazole, m.p. 171-172 °C, is 25 g (85%). Here limiting reagent is o-phenylenediamine; hence yield should be calculated from its amount taken.
How is a mono acyl derivative converted to a benzimidazole?
Mono acyl derivative of o-phenylenediamine is readily converted into the corresponding benzimidazole by the action of heat alone. These conversions are generally carried out at a temperature somewhat above the melting point of the starting compounds.
Is the benzimidazole a biologically active compound?
Benzimidazole nucleus is one of the bioactive heterocyclic compounds that exhibit a range of biological activities. Specifically, this nucleus is a constituent of vitamin B12 (O'Neil et al., 2001).The pharmacological activities of the benzimidazole containing moiety have been well documented (Amari et al., 2002).
How is the recrystallisation of benzimidazole done?
Recrystallisation: Dissolve the synthesized product in 400 ml of boiling water, add 2 g of decolourising carbon and digest for 15 min. Filter rapidly through a preheated Buchner funnel and a flask at the pump. Cool the filtrate to about 10 °C, filter off the benzimidazole, wash with 25 ml of cold water and dry at 100 °C.
Last Update: Oct 2021
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